【英文标准名称】:StandardTestMethodforEstimationofEngineOilVolatilitybyCapillaryGasChromatography
【原文标准名称】:用毛细管气相色谱法评定发动机油挥发性的标准试验方法
【标准号】:ASTMD6417-2003
【标准状态】:现行
【国别】:
【发布日期】:2003
【实施或试行日期】:
【发布单位】:美国材料与试验协会(US-ASTM)
【起草单位】:D02.04.0H
【标准类型】:(TestMethod)
【标准水平】:()
【中文主题词】:润滑剂;发动机油;润滑油;气相色谱法;石油;散热性;化学分析和试验;化工技术
【英文主题词】:boilingrangedistribution;engineoil,volatility;gaschromatography;lubricants;petroleum;simulateddistillation;volatility
【摘要】:Thedeterminationofengineoilvolatilityat371x00B0;C(700x00B0;F)isarequirementinsomelubricantspecifications.ThistestmethodisintendedasanalternativetoTestMethodsD5800andD5480andtheNoackmethodforthedeterminationofengineoilvolatility(seeDIN51.581).ThedataobtainedfromthistestmethodarenotdirectlyequivalenttoTestMethodD5800.Thecalculatedresultsoftheoilvolatilityestimationbythistestmethodcanbebiasedbythepresenceofadditives(polymericmaterials),whichmaynotcompletelyelutefromthegaschromatographiccolumn,orbyheavierbaseoilsnotcompletelyelutingfromthecolumn.Theresultsofthistestmethodmayalsonotcorrelatewithotheroilvolatilitymethodsfornonhydrocarbonsyntheticoils.Thistestmethodcanbeusedonlubricantproductsnotwithinthescopeofothertestmethodsusingsimulateddistillationmethodologies,suchasTestMethodD2887.1.1Thistestmethodcoversanestimationoftheamountofengineoilvolatilizedat371176;C(700176;F).1.1.1Thistestmethodcanalsobeusedtoestimatetheamountofoilvolatilizedatanytemperaturebetween126and371176;C,ifsodesired.1.2Thistestmethodislimitedtosampleshavinganinitialboilingpoint(IBP)greaterthan126176;C(259176;F)orthefirstcalibrationpointandtosamplescontaininglubricantbaseoilswithendpointslessthan615176;C(1139176;F)orthelastn-paraffinsinthecalibrationmixture.Byusingsomeinstrumentsandcolumns,itispossibletoextendtheusefulrangeofthetestmethod.1.3Thistestmethodusestheprinciplesofsimulateddistillationmethodology.1.4Thistestmethodmaybeappliedtobothlubricantoilbasestocksandfinishedlubricantscontainingadditivepackages.Theseadditivepackagesgenerallycontainhighmolecularweight,non-volatilecomponentsthatdonotelutefromthechromatographiccolumnunderthetestconditions.Thecalculationprocedureusedinthistestmethodassumesthatallofthesampleelutesfromthecolumnandisdetectedwithuniformresponse.Thisassumptionisnottrueforsampleswithnonvolatileadditives,andtheresultsmightbebiasedhighrelativetoTestMethodD5480,whichusesaninternalstandardtoaccountfortheunelutedmaterial.Forthisreason,resultsbythistestmethodarereportedasareapercentofoil.1.5ThevaluesstatedinSIunitsaretoberegardedasstandard.Thevaluesstatedininch-poundunitsareprovidedforinformationonly.1.6Thisstandarddoesnotpurporttoaddressallofthesafetyconcerns,ifany,associatedwithitsuse.Itistheresponsibilityoftheuserofthisstandardtoestablishappropriatesafetyandhealthpracticesanddeterminetheapplicabilityofregulatorylimitationspriortouse.
【中国标准分类号】:E34
【国际标准分类号】:75_100(LUBRICANTS,INDUSTRIALOILSANDRELATEDPRODUCTS)
【页数】:9P.;A4
【正文语种】:


MIL-STD-961C, MILITARY STANDARD: MILITARY SPECIFICATIONS AND ASSOCIATED DOCUMENTS, PREPARATION OF (20 MAY 1988)., This standard establishes the formats, contents, and procedures for the preparation of the military specification and its associated documents, prepared either by Government activities or under contract.